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LCMS (ESI-MS) analysis was performed using an Agilent HPLC system (1100 series) with a CC 125/4 Nucleodur C18 gravity column (3 m) from Macherey Nagel coupled to a Thermo Scientific Finnigan LCQ Advantage Max Ion Trap and ESA Corona detector

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Cloudiness, particles, or discoloration are signs of degradation or contamination

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