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Samples (1 l) were loaded onto a Zorbax 300SB C-18 Nano-HPLC Chip (150 mm75 m, Agilent) with 0.1%(v/v) formic acid (0.6 l/min), and compounds eluted by an increasing 0.1%(v/v) formic acid, acetonitrile gradient (90%(v/v) final)

doi: 10.1111/j.1365-2125.2011.03911.x 220 GuptaBLeVeaCLitwinAFakihMG

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10.1016/j.tiv.2022.105350