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The reaction was stopped by the addition of 0.1 mL of TCA and the mixture was centrifuged at 10,000 g for 10 min

N Engl J Med (2023) 389(10):87788

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L., et al., Alpha-lipoic acid induces adipose triglyceride lipase expression and decreases intracellular lipid accumulation in HepG2 cells